
1260
Analizador de Impedancia
Introducción
El
Analizador Solartron 1260 de Fase/Ganancia es sin duda el Analizador de
Respuesta de Frecuencia y de Impedancia/Fase-Ganancia más potente, preciso y
flexible que disponible hoy. Es usado diariamente por los investigadores
principales donde son una prioridad la fiabilidad experimental e integridad
de las medidas.
La sólida reputación del 1260A es respaldada frecuentemente
en trabajos publicados en campos tan diversos como:
• Corrosion studies.
•
Battery research and fuel cells.
•
Solar cells.
•
LCDs.
•
Bio-materials.
•
Dental research.
•
Electronic component development.
•
Civil engineering.
•
Coatings research.
•
Composite materials.
Part of
Solartron's extensive range of precision products designed to provide
cost-effective solutions for dc and ac analysis
in electrochemical and
materials research, 1260 offers an outstanding measurement specification for
impedance spectroscopy.
Benefits/Features:
• Frequency range 10microHz to 32MHz.
•
Frequency resolution: 1 in 65million (0.015ppm).
•
0.1%, 0.1° accuracy.
•
Resolution to 0.001dB, 0.01°.
•
Measures impedances >100Mohms.
•
2-, 3- and 4-terminal measurement configurations.
•
Polarization voltage up to ±40.95V.
•
Automatically sweeps frequency, amplitude or bias.
•
Null, normalize and auto-impedance modes.
•
Gain, phase, group delay and impedance measurements.
•
Built in statistical analysis.
•
Displays a,b,r,q,t,Z,R,X,Y,G,B,L,C,Q,D,D%.
•
Operates standalone or within a computer-controlled system.
•
Renowned Zplot software package simplifies experiments and optimizes
throughput.
Aplicaciones:
- Dielectric loss angle measurement for insulators
- Effects of moisture and aging in transformer oils
- Conduction mechanisms in ceramics for fuel cells and solid electrolytes
- Optimization of sensor mechanisms in gas detectors
- Biological organ and tissue studies
- Prediction of strength and hardness of concrete
- Curing of epoxy resins
- Strength of composite materials
- Dental research
- Liquid crystal display (LCD) research
Medidas de Impedancia
Virtually every liquid and
solid is able to pass current when a voltage is applied to it. If a variable
(ac) voltage is applied to the material, the ratio voltage to current (V/I)
is known as the impedance. In many materials, especially those which are not
generally regarded as conductors of electricity, the impedance varies with
the frequency of the applied voltage changes, in a way that is related to the
properties of the liquid or solid. This may be due to the physical structure
of the material, to chemical processes within it, or to a combination of
both. Thus, if a measurement of impedance over a suitable frequency range is
made, and the results plotted on suitable axes, it is possible to relate the
results to the physical and chemical properties of the material.
Since
impedance measurement is repeatable and non-destructive, it can provide
valuable insights into the behavior of a huge variety of substances,
components and systems.
For example, measuring the impedance of a sample of concrete can yield
information about the water content and proportions of the constituents,
leading to an estimate of the final strength of the material. Again, the
impedance plot of a sample of organic tissue - anything from a piece of fruit
to a human kidney - can reveal its condition and suitability for storage,
freezing or transplant.
The
advantages of impedance measurement over other techniques include:
• Rapid acquisition of data (often within minutes)
•
Accurate, repeatable measurements
•
Non-destructive
•
Highly adaptable to a wide variety of different applications.
Materials Characterization
The wide frequency range and superb
accuracy of the 1260 enables many different mechanisms to be investigated to
characterize material behavior, predict lifetime and failure rates, and for
improving fabrication and curing processes.
Particular
benefits of using 1260 for materials investigations include:
• Direct measurement of impedance from 10mohms to
>100Mohms
•
Null and normalize functions eliminate effects of leads and sample chambers
•
DC polarization up to ±40.95V
•
Wide frequency range covers most applications
•
Unsurpassed resolution can reveal small but critical changes in material
behavior
•
Wide range of display and output formats
•
Can form the heart of a dielectric test system to extend impedance
measurement into Gohm range.
LabView
drivers are available for the 1260 FRA from
National Instruments
Especificaciones
|
Generador
|
Modo Voltaje
|
Modo Corriente
|
|
Amplitud
AC
|
|
|
|
- para frequencias < 10MHz
|
0 a 3V rms
|
0 a 60mA rms
|
|
- para frequencias > 10 MHz
|
0 a 1V rms
|
0 a 2mA rms
|
|
Máxima resolución AC
|
5mV
|
100µA
|
|
Rango Polarización DC
|
±40.95V
|
±100mA
|
|
Resolución DC máxima
|
10mV
|
200µA
|
|
Impedancia de salida
|
50W ±1%
|
>200kW a <1kHz
|
|
Frecuencia
|
|
|
- rango
|
10µHz a 32 MHz
|
|
- Resolución máxima
|
10µHz
|
|
- error
|
±100ppm
|
|
- estabilidad, 24 horas
± 1ºC
|
±10ppm
|
|
Tipos de barridos
|
Frecuencia (log o lin), voltaje AC, voltaje DC, corriente AC, corriente
DC
|
|
Voltaje máximo
|
|
|
- Hi a Lo
|
±46V peak
|
|
- Lo a tierra
|
±0.4V peak
|
|
Corriente máxima
|
±100mA peak
|
|
Impedancia
|
|
|
Medida de Impedancia
|
>100 Mohms*
|
|
- Lo a tierra
|
100kW, <10nF
|
|
Conexión
|
Single BNC, Floating shield
|
|
Output
disable
|
Contact closure or
TTL logic 0
|
|
Entradas
|
Voltaje (2×)
|
Corriente
|
|
Rangos
|
30mV, 300mV, 3V
|
6µA, 60µA, 6mA, 60mA
|
|
Resolución Máxima
|
1µV
|
200pA
|
|
Full scale peak
|
±5V
|
±100mA
|
|
Entradas protegidas hasta
|
±46V
|
±250mA
|
|
Conexión
|
Single/Differential BNC
|
Single BNC
|
|
Pantallas
|
Floating/Grounded
|
-
|
|
Acoplamiento
|
DC o AC (-3dB a 1Hz)
|
DC o AC (-3dB a 1Hz)
|
|
Impedancia de
Entrada
|
|
|
|
- hi a pantalla
|
1Mohm, <35pF
|
³600µA rango, 1W
|
|
- Pantalla a tierra
|
10kohm, 330pF
|
<600µA rango,
50W
|
Límites de error
Ambient temperature 20 ± 10ºC, integration time, >200ms. Data valid for
one year after calibration.
Gain - Phase Measurements
Applies to all ranges at >10% full scales.
Results
Variable
- Frequency
- AC amplitude
- DC bias
Parámetros Medidos
- Voltage Gain
- Phase
- Real
- Imaginary
- Z, R, X, Y, G, B, V, I
- Group delay
- C, L, Q, D
Medidas de impedancia
Applies for stimulation level 1V for impedances >50W or 20mA for
impedances <50W, using 12601A.
Impedance Ranges (resolution 5 digits).
Medidas
de Impedancia: >100 Mohms*
Capacidad
- 1pF a 10mF
Resistencia
- 10mW a 100MW
Inductancia
- 100nH a 1000H
Interfaz
para conexión a PC
Usar NI-GPIB tipo PCI o adaptador USB/GPIB.
Software
ZPlot y
SetTemp para control de 1260 y Hornos con secuencias automáticas.
Celda portamuestras
GF-800 (800ºC) y
GF-1000 (1000ºC)
para medidas en sólidos a 2 o 4 electrodos, con paso de gas.
* Combinar con 1296 para mayores rangos de impedancia, hasta 100
TOhm.
|